Science Diliman, Vol 14, No 1 (2002)

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Synthesis of Bulk Superconducting Magnesium Diboride

Margie Olbinado, Leandro Jose Guerra, Rolando Sarmago

Abstract


Bulk polycrystalline superconducting magnesium diboride, MgB2, samples were successfully prepared via a one-step sintering program at 750°C, in pre Argon with a pressure of 1atm. Both electrical resistivity and magnetic susceptibility measurements confirmed the superconductivity of the material at 39K, with a transition width of 5K. The polycrystalline nature, granular morphology, and composition of the sintered bulk material were confirmed using X-ray diffractometry (XRD), scanning electron microscopy (SEM), and energy dispersive X-ray analysis (EDX).

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